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1.
A multi-analytical approach for the study of brazilwood and its lake pigments was carried out based on historically accurate reconstructions. Recipes for brazilwood lakes from the fifteenth century technical text Livro de como se fazem as cores and the Winsor & Newton nineteenth century colourman's archive were reproduced and compared. Both primary sources allowed for the successful preparation of brazilwood lake pigments with colours that vary from light pink to dark red. The main steps and ingredients for the manufacture of these pigments were common in both sources, particularly the addition of Al3+ in the form of alum, and calcium carbonate (chalk). Reconstructions revealed that the latter acts as a pH buffer and filler, controlling the pH at which the lake pigment precipitates. The main difference between the two sources is that the nineteenth century recipes give the quantities for all ingredients, the precise temperatures and time, and achieved higher relative pigment yields (75% versus 45%). Full chemical characterisation of the reconstructions provided detailed information on the individual steps in the pigment manufacture and revealed that the presence of calcium sulphate dihydrate (gypsum) in the final pigment was a result of its formation in situ. Infrared, reflectance, and fluorescence spectroscopy proved to be essential and complementary techniques: while infrared was used to characterise additives and binders, reflectance and fluorescence data were fundamental for identifying the chromophore. The pigments and paints produced can now be used as standards for the identification and investigation of brazilwood lake pigments found in artworks. 相似文献
2.
朱万强 《遵义师范学院学报》2006,8(5):58-60
考察和比较了一系列的原子灰颜填料的作用和功能及对原子灰固化的影响,发现重晶石粉料对不饱和聚酯树腊及原子灰的固化有明显的影响。 相似文献
3.
天然甘蓝食用色素化学稳定性研究 总被引:3,自引:0,他引:3
蔬菜花色素是天然食用色素中的一个主要类别,属水溶性色素.甘蓝色素是蔬菜花色素中新近开发的一种.本文测定了甘蓝色素吸收光谱和其在溶液中呈现红紫色的适宜酸度条件,观察了不同pH对该色素的影响和这些添加剂存在下它的光照稳定性.为甘蓝色素的开发应用提供了依据. 相似文献
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5.
Méndez A Pérez C Montañéz JC Martínez G Aguilar CN 《Journal of Zhejiang University. Science. B》2011,12(12):961-968
The combined effects of pH and temperature on red pigment production and fungal morphology were evaluated in a submerged culture
of Penicillium purpurogenum GH2, using Czapek-Dox media with d-xylose as a carbon source. An experimental design with a factorial fix was used: three pH values (5, 7, and 9) and two temperature
levels (24 and 34 °C) were evaluated. The highest production of red pigment (2.46 g/L) was reached with a pH value of 5 and
a temperature of 24 °C. Biomass and red pigment production were not directly associated. This study demonstrates that P. purpurogenum GH2 produces a pigment of potential interest to the food industry. It also shows the feasibility of producing and obtaining
natural water-soluble pigments for potential use in food industries. A strong combined effect (p<0.05) of pH and temperature was associated with maximal red pigment production (2.46 g/L). 相似文献
6.
采用冷浸提取、超声波提取及索氏提取法进行研究金鸡菊色素的含量,从而避免了单一方法的局限性。结果表明,超声波提取方法在粗提中显示明显的优势。于此同时,金鸡菊色素具有很好的抗氧化性,并且具有剂量效应关系,在光照和空气下该色素稳定性差,应避光保存。 相似文献
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为了研究“红花末”色素的理化特性及食用安全性,采用光谱法分析其吸收图谱及光稳定性和热稳定性,并利用小鼠急性毒性试验、小鼠精子畸变试验等方法进行毒理学研究.结果表明,“红花末”色素溶液在200~800 nm有5个吸收峰,可见区最大吸收峰为540 nm.色素光稳定性较差,热稳定性较好.急性毒性试验表明,“红花末”色素对小鼠的LD50值为1259 mg/kg&#183;bw,属于低毒级;遗传毒性试验表明:小鼠精子畸变率为8.38%~12.26%,明显高于对照组(0.54%,p&lt;0.05).“红花末”色素稳定性较好,属于低毒级,具有一定的致突变性,长期食用可能会对生殖系统产生一定的影响. 相似文献
9.
以D-101树脂为吸附材料,研究不同条件下对蛇莓果实红色素的吸附和解吸性能.研究发现:静态吸附中上样液温度为30℃时的吸附量较大;动态吸附中上样液酸度为0.5%,吸光度0.179~0.224, pH1.0,流速2 mL/min时的吸附量大;用80%乙醇以2 mL/min的流速进行洗脱时,解吸效果最好;蛇莓果实色素纯化后色价提高了3倍左右,该研究条件科学合理,纯化效果很好. 相似文献
10.
实验研究石斑木果皮红色素的理化性质和光、温度、金属离子、食品添加剂等对色素稳定性的影响.结果表明:该色素在80℃以下较稳定;日光照射,金属离子K^+、Na^+、Mg^2+、Ca^2+、Cu^2+、Mn^2+、Fd^3+等对色素液的吸光度有明显的不良影响;高浓度VitC和柠檬酸对色素降色明显;蔗糖和苯甲酸钠对色素无较大影响. 相似文献